广东LECO氧氮氢分析仪优惠价格

Method Selection

Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.

可选具有压力补偿和温度控制性能的标气检测气路。广东LECO氧氮氢分析仪优惠价格

Sample Preparation

Sampling and sample preparation is an important issue because traditional methods used to obtain samples for oxygen and nitrogen determination are different from those recommended for hydrogen, especially when sampling molten metal. The main difference in steel sampling procedures for oxygen/nitrogen and hydrogen is due to the mobilityof hydrogen. Special precautions must be used when sampling for hydrogen. From molten steel and iron, a sample must be quickly quenched in cold water and chilled in a refrigerant such as liquefied nitrogen or a mixture of acetone and solid carbon dioxide in order to reduce losses of hydrogen from diffusion. Losses of oxygen and nitrogen from diffusion are not a problem. A sample that is taken for hydrogen and

chilled in a refrigerant can also be used for oxygen and nitrogen determination. However, a sample that is typically taken for oxygen and/or nitrogen determination is not suitable for hydrogen determination due to hydrogen loss (diffusion). Surface contamination must be removed by filing or light grinding, using care not to overheat the sample.

浙江美国分析仪优惠价格***电极炉头设计，提高脉冲炉热交换效率。

Determine the instrument blank.

a. Login a minimum of 3 Blank replicates.

b. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

c. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

d. Clean the upper and lower electrode manually, or, if applicable, remove thecrucible and press the analyze button to clean with the automatic cleaner.

e. Firmly place a graphite crucible on the lower electrode tip.

f. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and endautomatically.

g. Repeat steps 2b through 2f a minimum of three times.

h. Set the blank following the procedure outlined in the operator's instruction manual.

Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Calibrate/drift following the procedure outlined in the operator's instruction manual.

Login Sample with the appropriate number of reps.

Weigh approximately *** grams of appropriately prepared sample into a *** Nickel Capsule, enter mass and sample identification into appropriate rep fields. If applicable, place the nickel capsule in the

appropriate autoloader position.

Repeat steps 3c through 3i for sample analysis.

美国LECO力可氧氮氢分析仪ONH836（氧氮氢联测仪）系列硬件部分

特点和优势

1、炉头区域LED照明系统

2、炉头快速拆装的粉尘过滤装置

3、装有自动旁路阀的可快速拆装氧水捕集装置

4、**的动态流量补偿（DFC）保证热导池气体流量、压力恒定

5、改进的红外检测池技术

     新红外池的恒温绝热技术消除了外界环境温度的干扰

   长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定

   氧高低双量程采用3个碳红外检测器，同时检测一氧化碳和二氧化碳，保证准确定量

  6、高效脉冲炉冷却系统

   强力内循环水冷装置

   双直流风扇保证持续冷却，不受电压波动的影响

   新电极炉头设计，提高脉冲炉热交换效率

  7、全自动分析系统（可选）

   自动清扫装置

   20位或100位全自动分析系统

   高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中，消除环境污染

改进的红外检测池技术。山西专业分析仪厂家供应

无需人工干预的全自动清扫系统。广东LECO氧氮氢分析仪优惠价格

Instrument calibration/drift correction.

a. Login a minimum of 3 Standard replicates.

b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.

c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

d. Place the calibration/drift standard into the open port at the top of the loading head.

e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

广东LECO氧氮氢分析仪优惠价格

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