北京LECO分析仪厂家报价

Determine the instrument blank.

a. Login a minimum of 3 Blank replicates.

b. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

c. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

d. Clean the upper and lower electrode manually, or, if applicable, remove thecrucible and press the analyze button to clean with the automatic cleaner.

e. Firmly place a graphite crucible on the lower electrode tip.

f. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and endautomatically.

g. Repeat steps 2b through 2f a minimum of three times.

h. Set the blank following the procedure outlined in the operator's instruction manual.

为可**的Cornerstone 氧氮氧分析软件采用触摸屏界面使用户达到分析控制、15法设定、在线诊断、数据报告。北京LECO分析仪厂家报价

Sample Preparation

Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.

江苏美国分析仪价格氧高低双量程采用3个碳红外检测一氧化碳和二氧化碳，保证准确定量。

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a

hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent

cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps

such as heat treating, pickling, and cleaning.

The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry. 

This application note was written specifically for use with the LECO ONH836 series determinator.

Method Selection

Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.

配置SmartLine® Remote远程诊断功能。

氧氮氢分析仪的优点

采用惰气熔融技术，同时测定氧、氮和氢元素含量

新设计封闭气路系统，优化气路循环，使氧氮氢测量更准确

可采用更廉价的氩气作为载气

催化炉温度可调，使氧的测量更加准确

气路系统都采用电磁阀控制，新增分段式漏气检测

水冷样品加样端口，有效隔绝杂质气体侵入

仪器配置和氧、氮、氢测量范围可灵活选择

新设计的高灵敏度红外检测池和热导池，有极低的检出限

分析时间短

脉冲炉功率高达8.5kw，温度3000℃

颗粒状样品无需胶囊包裹，使用经济实惠

化学试剂及管路隐藏在门后（可移除）

强大的分析软件（支持数据和应用报告导出、增加评论区及其他更多功能）。

单点和多点校正（线性回归）

可采用自来水、冷却循环水机或交换机冷却

新设计的产品可用于各类生产控制和实验室。

提供各种无机材料、钢铁、有色金属、硬质合金、陶瓷材料中宽范围的氧氮氢同时分析。北京LECO分析仪厂家报价

Procedure - Solid Samples

Prepare the instrument as outlined in the operator's instruction manual.

Determine the instrument blank.

Login a minimum of 3 Blank replicates.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Place a 502-344 Nickel Basket into the loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the

analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.

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