Procedure – Powder/Chip Samples
Determine the instrument blank.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
Add approximately 0.05 g of *** Graphite Powder to a 782-720 Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Sample Preparation
Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.
上海美国LECO分析仪用户友好界面的Cornerstone™ 软件。
Oxygen, Nitrogen, and Hydrogen in Refractory Metals
Summary
Oxygen and nitrogen are alloying elements in titanium, and are also classified as alpha stabilizing elements as they promote alpha phase alloys. Interstitial oxygen and nitrogen levels can be used to regulate the tensile strength of the material, but due to its high solubility can cause unwanted surface embrittlement. This phenomenon can be leveraged,however, under controlled processing to create surface films that increase surface hardness and wear properties.
美国LECO力可氧氮氢分析仪ONH836(氧氮氢联测仪)系列硬件部分
特点和优势
1、炉头区域LED照明系统
2、炉头快速拆装的粉尘过滤装置
3、装有自动旁路阀的可快速拆装氧水捕集装置
4、**的动态流量补偿(DFC)保证热导池气体流量、压力恒定
5、改进的红外检测池技术
新红外池的恒温绝热技术消除了外界环境温度的干扰
长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定
氧高低双量程采用3个碳红外检测器,同时检测一氧化碳和二氧化碳,保证准确定量
6、高效脉冲炉冷却系统
强力内循环水冷装置
双直流风扇保证持续冷却,不受电压波动的影响
新电极炉头设计,提高脉冲炉热交换效率
7、全自动分析系统(可选)
自动清扫装置
20位或100位全自动分析系统
高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中,消除环境污染
为可**的Cornerstone 氧氮氧分析软件采用触摸屏界面使用户达到分析控制、15法设定、在线诊断、数据报告。
Determine the instrument blank.
a. Login a minimum of 3 Blank replicates.
b. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
c. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
d. Clean the upper and lower electrode manually, or, if applicable, remove thecrucible and press the analyze button to clean with the automatic cleaner.
e. Firmly place a graphite crucible on the lower electrode tip.
f. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and endautomatically.
g. Repeat steps 2b through 2f a minimum of three times.
h. Set the blank following the procedure outlined in the operator's instruction manual.
Cornerstone氢氧氮分析软件同时支持***的书记文档格式和可变的报告格式。江苏LECO分析仪优惠价格
高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中,消除环境污染。山东美国分析仪哪家好
Instrument calibration/drift correction.
a. Login a minimum of 3 Standard replicates.
b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.
c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
d. Place the calibration/drift standard into the open port at the top of the loading head.
e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
山东美国分析仪哪家好
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