Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Calibrate/drift following the procedure outlined in the operator's instruction manual.
Login Sample with the appropriate number of reps.
Weigh approximately *** grams of appropriately prepared sample into a *** Nickel Capsule, enter mass and sample identification into appropriate rep fields. If applicable, place the nickel capsule in the
appropriate autoloader position.
Repeat steps 3c through 3i for sample analysis.
Sample Preparation
Typically, titanium and zirconium samples are chemically etched to remove surface contamination when oxygen and nitrogen are determined. However, etching can introduce hydrogen into the sample.
ASTM method E 1409 "Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert
Gas Fusion Technique", as updated in 1996, permits either etching or abrading (filing) of the test specimen.
ASTM E 1447 "Determination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal
Conductivity/Infrared Detection Method" permits surface preparation by abrading (if necessary to remove
contamination). Differences in sample preparation present somewhat of a dilemma regarding simultaneous
determination of O, N, and H in titanium. However, abrading samples with a file to remove surface
contamination will yield accurate O, N, and H results. The ONH836 utilizes a high-power electrode furnace to quickly and efficiently release the target gases from within the sample, which allows for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.
广东美国LECO分析仪哪家好采用三个**的红外器检测氧含量,同时检测CO和CO2,然后在转化为CO2集中检测。力可ONH836氧氮氢分析仪
特点和优势
国际**的非色散红外及热导检测器 ,无移动部件,不需要手动调整
采用三个**的红外器检测氧含量,同时检测CO和CO2,然后在转化为CO2集中检测,原理上是**完善的,所以不仅可以保证中间量程的测量精度,在**含量和高含量的检测范围内同样可以满足精度要求
高性能的红外检测器配置***恒温绝热技术,消除了外界环境温度的干扰
长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性
力可**的动态流量补偿控制DFC系统,保证了流量系统的完善,可以精确控制整个气路中的流量,保持流量恒定**改善了材料中氮分析的准确度
可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性,使得分析结果更加准确
可选自动功能
20位试样自动进样系统
通用下电极坩埚支座,容纳各种坩埚使用
无需人工干预的全自动清扫系统
Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Add approximately 0.05 g of *** Graphite Powder to a***Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen,the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 3b through 3i a minimum of three times for each calibration/drift standard used.
减少了繁琐的额外数据处理。Procedure - Solid Samples
Determine the instrument blank.
Repeat steps 2b through 2g a minimum of three times.
Set the blank following the procedure outlined in the operator's instruction manual.
Instrument calibration/drift correction.
Login a minimum of 3 Standard replicates.
Weigh approximately *** grams of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.
Note: LECO Reference Materia***o not require preparation.See preparation statement on the reference material certificate.
提供各种无机材料、钢铁、有色金属、硬质合金、陶瓷材料中宽范围的氧氮氢同时分析。广东美国LECO分析仪哪家好
ONH836仪器通过***采纳客户的反馈意见和创新设计。浙江美国LECO氧氮氢分析仪优惠价格
Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
Place the Nickel Capsule containing the sample into the open port at the top of the loading head.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
上海禹重实业有限公司致力于仪器仪表,是一家服务型公司。公司业务分为光谱仪,色谱仪,质谱仪,样品前处理等,目前不断进行创新和服务改进,为客户提供良好的产品和服务。公司注重以质量为中心,以服务为理念,秉持诚信为本的理念,打造仪器仪表良好品牌。禹重科技凭借创新的产品、专业的服务、众多的成功案例积累起来的声誉和口碑,让企业发展再上新高。
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