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Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

Titanium is a metal that can be combined with elements such as aluminum, vanadium, molybdenum, and tin to produce high-strength, lowdensity, and corrosion-resistant alloys. Titanium alloys are used by the military, medical devices, sporting goods, and aerospace industries because of these properties, and due to the strict demands of these industries, effort needs to be taken to assure that the material meets the highest of quality standards.

全自动分析系统、打印机、天平、远程诊断。山西分析仪采购

Procedure - Solid Samples

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner

Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically

Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

Place the Nickel Capsule containing the sample into the open port at the top of the loading head.

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.

氧氮氢分析仪的常见故障及解决方法

供电正常、通讯正常，点击确认键后分析仪不工作。这是没有水流，炉子温度太高或仪器通道电压不正常。如没有水流，炉子温度太高这些信息会显示在显示器画面上，但没有信息显示说明这两项正常。接下来检查仪器通道零位电压，如果比±3V高出1V以上，可能是因为气瓶空了，或者是空气进入到分析仪中。检查并更换化学试剂，如果有空气进入热导池里，热导池的电压就会＜-6V，此时打开右面的门，堵住炉子气体进口，10s后，热导池电压值必然升高。经过逐一排查，**终确认碱石棉有问题，更换后仪器正常。 ***红外池的恒温绝热技术消除了外界环境温度的干扰。

仪器的亮点和优势：

特点和优势

·炉头区域LED照明系统

·炉头快速拆装的粉尘过滤装置

·装有自动旁路阀的可快速拆装氧水捕集装置

·**的动态流量补偿（DFC）保证热导池气体流量、压力恒定

高效脉冲炉冷却系统

·强力内循环水冷装置热交换效率

·双直流风扇保证持续冷却，不受电压波动的影响

·***电极炉头设计，提高脉冲炉

全自动分析系统（可选）

·自动清扫装置

·20位或100位全自动分析系统

·高效全自动真空除尘装置直接将粉尘排至仪器外部捕集器中，消除环境污染

改进的红外检测池技术

·***红外池的恒温绝热技术消除了外界环境温度的干扰

·长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定性

·氧高低双量程采用3个碳红外检测器同时检测一氧化碳和二氧化碳，保证准确定量 采用三个**的红外器检测氧含量，同时检测CO和CO2，然后在转化为CO2集中检测。上海专业元素分析仪厂家直销

Cornerstone氧氮氢分析软件同时支持***的数据文档格式和可变的报告格式。山西分析仪采购

Summary

The determination of the amount of oxygen, nitrogen, and hydrogen in iron, steel, nickel-, and cobalt-base alloys represents some of the most important quality metrics for these materials. Oxygen is used to create steel from pig iron by removing excess carbon. Oxygen content must be controlled to limit the amount of carbon monoxide that can be formed during solidification which may cause excessive porosity. Nitrogen is considered both an impurity as well as an important alloying agent. Itcan be present as a nitride or interstitially in its gaseous form. Increased nitrogen content is known to increase yield and tensile strength, thus decreasing ductility and formability. Excessive levels may evolve during solidification thus increasing porosity. High hydrogen content is the primary cause of embrittlement, blistering and flaking due to its high

mobility through the lattice and provides no potential alloying benefits. The ONH836 utilizes a high-power

electrode furnace to quickly and efficiently release the target gases from within the sample, which allows

for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.

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